Palladium CAS:7440-05-3 ʻEleʻele Pahu
| Helu Helu | XD90595 |
| inoa mea kūʻai | Palladium |
| CAS | 7440-05-3 |
| ʻĀpana Molekala | Pd |
| Kaumaha Molecular | 106.42 |
| Nā kikoʻī mālama | Ambient |
| Kānāwai Kūʻai Kūlike | 38151200 |
Huahana Huahana
| Ka nana aku | Pauda ʻeleʻele |
| Hoʻāʻo | 99% |
| Wai | 70% ka nui |
| IR | <0.001% |
| AS | 0.002% |
| Fe | <0.001% |
| Cu | <0.001% |
| Pb | <0.001% |
| Cd | <0.001% |
| Zn | 0.001% |
| Ni | 0.001% |
| Mg | <0.001% |
| Al | <0.001% |
| Si | <0.001% |
| Cr | <0.001% |
| Co | <0.001% |
| Pd | 4.95% |
| Sb | 0.001% |
| Mn | <0.001% |
| Pt | <0.001% |
| Rh | <0.001% |
| Au | <0.001% |
| Ag | <0.001% |
| Sn | 0.001% |
| Mo | <0.001% |
| Bi | <0.001% |
| Ti | <0.001% |
| W | 0.001% |
| Zr | <0.001% |
| V | <0.001% |
| Ru | <0.001% |
| ʻāpana ili kiko | >970m2/g |
Hōʻike ka hana i kēia manawa i kahi moʻolelo i hoʻokahi ʻanuʻu, ka protocol ʻōmaʻomaʻo no ka synthesis o ka starch-stabilized palladium nanoparticles (PdNPs) me ka awelika ʻāpana ʻāpana o 30-40 nm.Ua kūpaʻa kēia mau ʻāpana a ua like ka nui.Ma ka protocol i kēia manawa, ua hoʻokō ʻia ka hoʻemi ʻana o ka palladium chloride me ka hoʻohana ʻana i ka waikawa citric ma ke ʻano he mea hoʻemi a me ka starch ma ke ʻano he capping agent.UV-Visible spectroscopy, Transmission Electron Microscopy, Field Emission Gun-Scanning Electron Microscopy, Selected Electron Diffraction and Electron dispersive X-ray Spectral analysis techniques i hoʻohana ʻia no ke ʻano o kēia starch capped PdNPs.Eia;ke hōʻike nei mākou i ka hui pū ʻana o ka starch a me ka waikawa citric i ka synthesis o PdNPs no ka manawa mua.Ua nānā ʻia ka hana catalytic o nā nanoparticles synthesized no Suzuki a me Heck cross coupling reactions.Ua hōʻoia ʻia ka huahana e GC.Ua hōʻoia ʻia nā huahana me ka hoʻohana ʻana i ka loiloi GC-MS a me ka hoʻohana ʻana i ka GC me ka lp o nā kūlana ʻoiaʻiʻo.Ua hōʻike ʻia ka hana maikaʻi loa o nā PdNP i kōkua i ka ikehu o ka lā ma waena o nā aryl halides (I, Br) me ka waika phenyl boronic a me nā mea i loaʻa.Eia hou, ua hōʻike ka catalyst i ka hana maikaʻi ma ka Heck coupling reaction of CC bond form of aryl halides with aromatic alkene.ʻO ka hoʻohana ʻana i ka starch, citric acid, ka wai a me ka ikehu lā e ʻoi aku ka ʻōmaʻomaʻo o kēia manawa.
